Solid State Spectroscopy Practical
Lecturers: Mohammad Mangir Murshed
(I) In-situ (temperature) and ex-situ Fourier transform infrared (FTIR) spectroscopy on some given oxides followed by data analysis (mode assignment, frequency shift with respect to crystal chemistry).
(II) In-situ (temperature) and ex-situ Raman spectroscopy (Stokes and anti-Stokes) on some given compounds followed by data analysis (calculation of absolute temperature, mode assignment, frequency shift with respect to crystal chemistry, mode Grüneisen parameter) and modeling (phonon decay, mode anharmonicity, phonon confinement).
(III) In-situ (temperature) and ex-situ UV-Vis diffuse reflectance spectroscopy followed by data analysis (calculation of bandgap and types of bandgaps) and modeling.
(IV) In-situ (temperature) and ex-situ inelastic and quasi-elastic neutron scattering data analysis.
(V) In-situ (temperature) and ex-situ MAS NMR data analysis.
After attending the practical course (one of the above) the participants shall have the following skills:
- know basic parts of the instrument
- know how to set up the respective experiment
- know how to collect data followed by data analysis
- know how to correlate the spectral information to the complementary bulk analysis such as X-ray/neutron elastic scattering experiments
Lab performance (experiment setup, data collection, data analysis) followed by written report
Laborbericht
Hans Kuzmany: Solid-State Spectroscopy: An Introduction (Springer, Heidelberg, 2nd Edition, 2009)
Norman B. Colthup, Lawrence H. Daly, Stephen E. Wiberley: Introduction to Raman and Infrared Spectroscopy (Academic Press, San Diego, 1990)
Heinz-Helmut Perkampus: UV-VIS Spectroscopy and Its Applications (Springer, Heidelberg1992)
Melinda J. Duer: Introduction to Solid-State NMR Spectroscopy (Blackwell, Oxford, 2005)
Françoise Hippert, Erik Geissler, Jean Louis Hodeau, Eddy Lelièvre-Berna, Jean-René Regnard: Neutron and X-ray Spectroscopy (Springer, Berlin, 2006)
1st teaching week:
2nd teaching week:
3rd teaching week:
4th teaching week:
5th teaching week:
6th teaching week:
7th teaching week:
8th teaching week:
9th teaching week:
10th teaching week:
11th teaching week:
12th teaching week:
13th teaching week:
14th teaching week:
Basic Data
05-MCM-SO-2
Study Program
Master Materials Chemistry and Mineralogy
Module Name
Solid State Spectroscopy
Course Type
Practical Laboratory (LP)
First Year of Study
3 CP
2 SWS
Summer Term
Course Language
English